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Basic One- and Two-Dimensional NMR Spectroscopy, 4th Completely revised edition

ISBN-10:3-52731233-1
ISBN-13:978-3-52731233-7

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General descriptionA classic among NMR textbooks, this thoroughly enlarged and updated fourth edition includes polymer solid state NMR, analysis of biopolymers, and applications of Magnetic Resonance Tomography and Magnetic Resonance Spectroscopy. Written by an NMR expert with long-standing teaching experience, this text provides students and professionals with a lucidly written introduction to NMR spectroscopy. The book forms an excellent bridge between the very simple texts on spectral interpreataion and more specialist works with an emphasis on mathematical theory.

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publication infoH. Friebolin, John Wiley & sons, 2005, 430 pp., soft cover

Table Of Contents

Table of Contents1 The Physical Basis of NMR Spectroscopy.
1.1 Introduction.
1.2 Nuclear Angular Momentum and Magnetic Moment.
1.3 Nuclei in a Static Magnetic Field.
1.4 Basic Principles of the NMR Experiment.
1.5 The Pulsed NMR Method.
1.6 Spectral Parameters: a Brief Survey.
1.7 "Other" Nuclides.
2 The Chemical Shift.
2.1 Introduction.
2.2 1H Chemical Shifts of Organic Compounds.
2.3 13C Chemical Shifts of Organic Compounds.
2.4 Relationships between the Spectrum and the Molecular Structure.
2.5 Chemical Shifts of "Other" Nuclides.
3 Indirect Spin-Spin Coupling.
3.1 Introduction.
3.2 H,H Coupling Constants and Chemical Structure.
3.3 C,H Coupling Constants and Chemical Structure.
3.4 C,C Coupling Constants and Chemical Structure.
3.5 Correlations between C,H and H,H Coupling Constants.
3.6 Coupling Mechanisms.
3.7 Couplings of "Other" Nuclides (Heteronuclear Couplings).
4 Spectrum Analysis and Calculations.
4.1 Introduction.
4.2 Nomenclature.
4.3 Two-Spin Systems.
4.4 Three-Spin Systems.
4.5 Four-Spin Systems.
4.6 Spectrum Simulation and Iteration.
4.7 Analysis of 13C NMR Spectra.
5 Double Resonance Experiments.
5.1 Introduction.
5.2 Spin Decoupling in 1HNMR Spectroscopy.
5.3 Spin Decoupling in 13C NMR Spectroscopy.
6 Assignment of 1H and 13C Signals.
6.1 Introduction.
6.2 1HNMR Spectroscopy.
6.3 13C NMR Spectroscopy.
6.4 Computer-aided Assignment of 13C NMR Spectra.
7 Relaxation.
7.1 Introduction.
7.2 Spin-Lattice Relaxation of 13C Nuclei (T1).
7.3 Spin-Spin Relaxation (T2).
8 One-Dimensional NMR Experiments using Complex Pulse Sequences.
8.1 Introduction.
8.2 Basic Techniques Using Pulse Sequences and Pulsed Field Gradients.
8.3 The J-Modulated Spin-Echo Experiment.
8.4 The Pulsed Gradient Spin-Echo Experiment.
8.5 Signal Enhancement by Polarization Transfer.
8.6 The DEPT Experiment.
8.7 The Selective TOCSY Experiment.
8.8 The One-Dimensional INADEQUATE Experiment.
9 Two-Dimensional NMR Spectroscopy.
9.1 Introduction.
9.2 The Two-Dimensional NMR Experiment.
9.3 Two-Dimensional J-Resolved NMR Spectroscopy.
9.4 Two-Dimensional Correlated NMR Spectroscopy.
9.5 The Two-Dimensional INADEQUATE Experiment.
10 The Nuclear Overhauser Effect.
10.1 Introduction.
10.2 Theoretical Background.
10.3 Experimental Aspects.
10.4 Applications.
11 Dynamic NMR Spectroscopy (DNMR).
11.1 Introduction.
11.2 Quantitative Calculations.
11.3 Applications.
12 Shift Reagents.
12.1 Lanthanide Shift Reagents (LSRs).
12.2 Chiral Lanthanide Shift Reagents.
12.3 Chiral Solvents.
13 Macromolecules.
13.1 Introduction.
13.2 Synthetic Polymers.
13.3 Biopolymers.
14 NMR Spectroscopy in Biochemistry and Medicine.
14.1 Introduction.
14.2 Elucidating Reaction Pathways in Biochemistry.
14.3 High-Resolution in vivo NMR Spectroscopy.
14.4 Magnetic Resonance Tomography.
Subject Index.